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Old Nov 4th, 2009, 01:34 PM       
The most interesting experiment I ever did was observing the critical point of CO2. Preparation was a nightmare, but the actual experiment was pretty cool. The liquid/gas meniscus kind of "fizzles out" at just above 31°C, then as you reduce the temperature it "fizzles back in".

The most dangerous chemical I've worked with was "aqua regia". Nasty.
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